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      Expanding the chemistry of thiolyl derivatives of phospholes

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      SPMSG1000498G.pdf (1.049Mb)
      Author
      Lin, Yuhan
      Date of Issue
      2011
      School
      School of Physical and Mathematical Sciences
      Abstract
      Bis[(3,4-dimethylphosphole) Pentacarbonyltungsten] sulfide, 3 , the precursor of P-S-P linked phosphinidene, 2, undergoes a [2+2] cycloaddition, followed by a Cope rearrangement to form the [4+4] cycloaddition adduct, 5. The mechanism has been proven by the isolation and characterization of the [2+2] cycloaddition adduct, 4. From optimization of compound 5, it was found to work best with visible light irradiation using dichloromethane as the solvent.
      Subject
      DRNTU::Science
      Type
      Thesis
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      • SPMS Theses

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